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  • BSI
    BS EN ISO 10301:1997, BS 6068-2.58:1997 Water quality. Determination of highly volatile halogenated hydrocarbons. Gas-chromatographic methods
    Edition: 1997
    $418.55
    / user per year

Description of BS EN ISO 10301:1997 1997

This International Standard specifies two methods for the determination of highly volatile halogenated hydrocarbons using gas chromatography.

Section 2 specifies a method for the determination by liquid/liquid extraction of highly volatile halogenated hydrocarbons in drinking water, ground water, swimming pool water, most rivers and lakes and many sewage and industrial effluents. Typical values of "quantification limits" are given in table 1.

Table 1

Typical values of "quantification limits" for some highly volatile halogenated hydrocarbons using liquid/liquid extraction

Compound Quantification limits
μ9/l
Dichloromethane 50
Chloroform 0,05 - 0,3
Carbon tetrachloride o 0 1 p
1,1-Dichloroethane 1,0-5
1,2-Dichloroethane 5-10
1,1,1-Trichloroethane 0,02 - 0,1
1,1,2,2-T etrachloroethane 0,05 - 0,1
Hexachloroethane 0,01 - 0,05
cis-1,2-Dichloroethylene 5-50
trans,2-Dichloroethylene 1 - 10
Trichloroethylene 0,05-0,1
Tetrachloroethylene 0,1
Hexachlorobutadiene 0,01
Tribromomethane 0,1
1,1,2-Trichlorotrifluoroethane 0,1

Section 3 specifies a method for the determination of highly volatile halogenated hydrocarbons in drinking water, surface waters and ground water by a static headspace method. Typical values of "quantification limits" are given in table 2.

In practise, the head-space method is applicable for industrial effluents as a screening method, but in some cases it is necessary to confirm the result by the liquid-liquid extraction method.

NOTE: When applying this International Standard, the guide on analytical quality control for water analysis (see ISO/TR 13530) should be followed, especially for the calibration steps.

Table 2

Typical values of "quantification limits" for some highly volatile halogenated hydrocarbons using static head-space method

Compound Quantification limits
μ9/I
Dichloromethane 50
Chloroform 0,3
Carbon tetrachloride 0,1
1,1-Dichloroethane 100
1,2-Dichloroethane 100
1,1,1-Trichloroethane 0,1
1,1,2-Trichloroethane 20
1,1-Dichloroethylene 10
cis-1,2-Dichloroethylene 50
trans-1 ,2-Dichloroethylene 25
Trichloroethylene 0,2
Tetrachloroethylene 0,2
1,2-Dichloropropane 50
1,3-Dichloropropane 200
cis+ trans-1,3-Dichloropropylene 10
Dibromomethane 0,3
Tribromomethane (Bromoform) 5
1,2-Dibromoethane 2
Bromochloromethane 1
Bromodichloromethane 0,2
Dibromochloromethane 0,3
1,1,3-Trifluoroethane 1


Standard NumberBS EN ISO 10301:1997, BS 6068-2.58:1997
TitleWater quality. Determination of highly volatile halogenated hydrocarbons. Gas-chromatographic methods
StatusUnder Review
Publication Date1997-07-15
Identical National Standard OfEN ISO 10301:1997, ISO 10301:1997
DescriptorsWater, Quality, Solvent extraction methods, Interferences (chemical), Halogenated hydrocarbons, Water pollution, Haloalkanes, Identification methods, Water treatment, Calibration, Gas-liquid chromatography, Potable water, Test equipment, Chemical analysis and testing, Determination of content, Effluents (sewage), Sampling methods, Gas chromatography, Specimen preparation, Precision, Water testing, Test specimens, Surface water, Trade effluents, Ground water, Haloalkenes
ICS13.060.50 Examination of water for chemical substances
CommitteeEH/3/2
ISBN0 580 27541 8
PublisherBSI
Pages40

About BSI

BSI Group, also known as the British Standards Institution is the national standards body of the United Kingdom. BSI produces technical standards on a wide range of products and services and also supplies certification and standards-related services to businesses.
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