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  • BSI
    BS EN 62321-6:2015 Determination of certain substances in electrotechnical products - Polybrominated biphenyls and polybrominated diphenyl ethers in polymers by gas chromatography-mass spectrometry (GC-MS)
    Edition: 2015
    $497.46
    / user per year

Description of BS EN 62321-6:2015 2015

This Part of IEC 62321 specifies one normative and two informative techniques for the determination of polybrominated biphenyls (PBB) and diphenyl ethers (PBDE) in polymers of electrotechnical products.

The gas chromatography–mass spectrometry (GC-MS) test method is suitable for the determination of monobrominated to decabrominated biphenyls (PBB) and monobrominated to decabrominated diphenyl ethers (PBDE).

Annexes A and C contain methods using ion attachment mass spectrometry (IAMS) coupled with direct injection probe (DIP) and high-pressure liquid chromatography coupled to photo diode array ultra violet detector (HPLC-PDA/UV). These techniques have utility as fast, qualitative or semi-quantitative type methods but are subject to limitations including interferences or the number or type of PBB and PBDE compounds within their scope.

The ion attachment mass spectrometry (IAMS) technique is limited to the determination of decabromo biphenyl and technical mixtures of decabromodiphenyl ether, octabromodiphenyl ether, and pentabromo diphenyl ether flame retardant compounds. The determination of other PBBs or PBDEs by this method has not been evaluated.

The high-pressure liquid chromatography technique is limited to the determination of technical mixtures of decabromodiphenyl ether, octabromo diphenyl ether, decabromo biphenyl and octabromo biphenyl technical flame retardants. The determination of other PBBs or PBDEs by this method has not been evaluated.

These test methods have been evaluated for use with PS-HI (polystyrene, high-impact) and PC/ABS (a blend of polycarbonate and acrylonitrile butadiene styrene) containing individual PBDEs between 20 mg/kg to 2 000 mg/kg and total PBDEs between 1 300 mg/kg to 5 000 mg/kg as depicted in this standard including in Annex F. The use of these methods for other polymer types, PBBs or other PBDE compounds or concentration ranges other than those specified above has not been specifically evaluated.



Standard NumberBS EN 62321-6:2015
TitleDetermination of certain substances in electrotechnical products - Polybrominated biphenyls and polybrominated diphenyl ethers in polymers by gas chromatography-mass spectrometry (GC-MS)
StatusDefinitive
Publication Date2015-10-31
ReplacesBS EN 62321:2009
Identical National Standard OfEN 62321-6:2015, IEC 62321-6:2015
DescriptorsLead, Cadmium, Mercury, Electrical equipment, Electronic equipment and components, Chemical analysis and testing, Dangerous materials, Electrical components, Environmental engineering, Determination of content, Biphenyl, Chromium, Flame retardants
ICS43.040.10 Electrical and electronic equipment, 13.020.01 Environment and environmental protection in general
CommitteeGEL/111
ISBN978 0 580 74396 2
PublisherBSI
Pages64

About BSI

BSI Group, also known as the British Standards Institution is the national standards body of the United Kingdom. BSI produces technical standards on a wide range of products and services and also supplies certification and standards-related services to businesses.
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