1. Scope

1.1 This test method covers determination of surface area of metal powders. The test method specifies general procedures that are applicable to many commercial physical adsorption instruments. The method provides specific sample outgassing procedures for listed materials. It includes additional general outgassing instructions for other metals. The multipoint equation of Brunauer, Emmett and Teller (BET), along with the single point approximation of the BET equation, forms the basis for all calculations.

1.2 This test method does not include all existing procedures appropriate for outgassing metallic materials. The procedures included provided acceptable results for samples analyzed during interlaboratory testing. The investigator shall determine the appropriateness of listed procedures.

1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.3.1 State all numerical values in terms of SI units unless specific instrumentation software reports surface area using alternate units. In this case, present both reported and equivalent SI units in the final written report. Many instruments report surface area as m ² /g, instead of using correct SI units (m ² /kg).

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

ASTM Standards

B215 Practices for Sampling Metal Powders

B243 Terminology of Powder Metallurgy

E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method

Keywords

BET surface area; metal powders; multipoint surface area; outgassing; physical adsorption; refractory metal powders; single point surface area; specific surface area; surface area; BET (Brunauer, Emmett, and Teller) surface area; Metal powders; Multipoint surface area; Outgassing materials/processes; Physical adsorption; Refractory metal powders; Single-point surface area; Specific surface area; Surface analysis--metals/alloys;

ICS Code

ICS Number Code 77.160 (Powder metallurgy)

DOI: 10.1520/B0922-02R08

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