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eLibrary > BS ISO 29301:2023 Microbeam analysis. Analytical electron microscopy. Methods for calibrating image magnification by using reference materials with periodic structures >

BS ISO 29301:2023 Microbeam analysis. Analytical electron microscopy. Methods for calibrating image magnification by using reference materials with periodic structures, 2023

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BS ISO 29301:2023 Microbeam analysis. Analytical electron microscopy. Methods for calibrating image magnification by using reference materials with periodic structures, 2023

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Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Image magnification [Go to Page]
4.1 Definition of the image magnification
4.2 Expressing magnification
5 Reference materials [Go to Page]
5.1 General
5.2 Requirements for CRM/RM
5.3 Storage and handling
6 Calibration procedures [Go to Page]
6.1 General
6.2 Mounting CRM/RM
6.3 Setting TEM operating conditions for calibration
6.4 Capturing digitized image
6.5 Digitizing the image recorded on photographic film [Go to Page]
6.5.1 General
6.5.2 How to decide the pixel-resolution for digitization
6.6 Measurement of the angle-corrected distance, Dt, from the digitized image [Go to Page]
6.6.1 General
6.6.2 Measurement procedure
6.7 Digitization of reference scale for pixel size calibration
6.8 Calibration of image magnification [Go to Page]
6.8.1 General
6.8.2 Calibration of scale unit (= pixel size), S
6.8.3 Calculating image magnification
6.9 Calibration of scale bar [Go to Page]
6.9.1 General
6.9.2 Basic scale size corresponding to one pixel on the digitized image
6.9.3 Calibration of scale bar
6.10 Calibration procedure for length measurements using photographic film only
7 Accuracy of image magnification
8 Uncertainty of measurement result
9 Calibration report [Go to Page]
9.1 General
9.2 Contents of calibration report
Annex A (informative) Parameters that influence the resultant magnification of a TEM
Annex B (informative) Flowchart of image-magnification calibration procedure
Annex C (informative) How to decide the number of lines for averaging
Annex D (informative) Reference materials for magnification calibration
Annex E (informative) Example of test report for calibration of TEM magnification
Bibliography [Go to Page]

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BS ISO 29301:2023 Microbeam analysis. Analytical electron microscopy. Methods for calibrating image magnification by using reference materials with periodic structures, 2023

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