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  • BSI
    BS EN 16694:2015 Water quality. Determination of selected polybrominated diphenly ether (PBDE) in whole water samples. Method using solid phase extraction (SPE) with SPE-disks combined with gas chromatography-mass spectrometry (GC-MS)
    Edition: 2015
    $418.55
    / user per year

Description of BS EN 16694:2015 2015

This European Standard specifies a method for the determination of six selected polybrominated diphenyl ethers (PBDE) listed in Table 1, representative for technical brominated diphenyl ethers (BDE) in water samples in mass concentrations ≥ 0,025 ng/l for each individual congener. The method uses solid-phase extraction with SPE-disks in combination with gas chromatography-mass spectrometry (GC-MS). It is applicable to the analysis of PBDE in surface water containing suspended particulate matter (SPM) up to 500 mg/l (whole water samples), drinking water and groundwater. The limit of quantification (LOQ) was determined according to ISO/TS 13530, on the basis of replicate determinations of the procedural blank, carried out under reproducibility conditions.

This method may be used for the analysis of other BDE congeners not listed in Table 1 or other types of water. However, it is important to verify its applicability before use.

Table 1 — Polybrominated diphenyl ethers (PBDE) determined by this method

Congener Abbreviationa Formula Molar mass g/mol CAS RNb
2,4,4’-Tribromodiphenyl ether BDE-28 C12H7Br3O 406,8954 41318–75–6
2,2’,4,4’-Tetrabromodiphenyl ether BDE-47 C12H6Br4O 485,7950 5436–43–1
2,2’,4,4’,5-Pentabromodiphenyl ether BDE-99 C12H5Br5O 564,6911 60348–60–9
2,2’,4,4’,6-Pentabromodiphenyl ether BDE-100 C12H5Br5O 564,6911 189084–64–8
2,2’,4,4’,5,6’-Hexabromodiphenyl ether BDE-154 C12H4Br6O 643,5872 68631–49–2
2,2’,4,4’,5,5’-Hexabromodiphenyl ether BDE-153 C12H4Br6O 643,5872 207122–15–4

NOTE EC numbers are not applicable for PBDE congeners.

a Numbering analog to IUPAC nomenclature for PCB

b CAS RN: Chemical Abstracts Service Registry Number


Standard NumberBS EN 16694:2015
TitleWater quality. Determination of selected polybrominated diphenly ether (PBDE) in whole water samples. Method using solid phase extraction (SPE) with SPE-disks combined with gas chromatography-mass spectrometry (GC-MS)
StatusConfirmed
Publication Date2015-09-30
Identical National Standard OfEN 16694:2015
DescriptorsWater, Chromatography, Extraction methods of analysis, Determination of content, Water testing, Polynuclear aromatic hydrocarbons, Aromatic hydrocarbons, Fluorimetry, Potable water, Thin-layer chromatography, Quality, Chemical analysis and testing
ICS13.060.50 Examination of water for chemical substances
CommitteeEH/3/2
ISBN978 0 580 84520 8
PublisherBSI
Pages36

About BSI

BSI Group, also known as the British Standards Institution is the national standards body of the United Kingdom. BSI produces technical standards on a wide range of products and services and also supplies certification and standards-related services to businesses.
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