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  • ASTM
    C696-19 Standard Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Uranium Dioxide Powders and Pellets
    Edition: 2019
    $78.62
    Unlimited Users per year

Description of ASTM-C696 2019

ASTM C696-19

Active Standard: Standard Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Uranium Dioxide Powders and Pellets




ASTM C696

Scope

1.1 These test methods cover procedures for the chemical, mass spectrometric, and spectrochemical analysis of nuclear-grade uranium dioxide powders and pellets to determine compliance with specifications.

1.2 Units—The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.

1.3 The analytical procedures appear in the following order:

 

Sections

 

Uranium by Ferrous Sulfate Reduction in Phosphoric Acid and Dichromate Titration Method

2

Uranium and Oxygen Uranium Atomic Ratio by the Ignition (Gravimetric) Impurity Correction Method

3

Carbon (Total) by Direct Combustion-Thermal Conductivity Method

2

Total Chlorine and Fluorine by Pyrohydrolysis Ion-Selective Electrode Method

3

Moisture by the Coulometric, Electrolytic Moisture Analyzer Method

8 – 15

Nitrogen by the Kjeldahl Method

16 – 23

Isotopic Uranium Composition by Multiple-Filament Surface Ionization Mass Spectrometric Method

4

Spectrochemical Determination of Trace Elements in High-Purity Uranium Dioxide

5

Silver, Spectrochemical Determination of, by Gallium Oxide Carrier D-C Arc Technique

5

Rare Earths by Copper Spark-Spectrochemical Method

2

Impurity Elements by a Spark-Source Mass Spectrographic Method

2

Surface Area by Nitrogen Absorption Method

24 – 30

Total Gas in Reactor-Grade Uranium Dioxide Pellets

2

Thorium and Rare Earth Elements by Spectroscopy

2

Hydrogen by Inert Gas Fusion

3

Uranium Isotopic Analysis by Mass Spectrometry

2

1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.


Keywords

impurity content; isotopic composition; stoichiometry; uranium content; uranium dioxide;


ICS Code

ICS Number Code 27.120.30 (Fissile materials and nuclear fuel technology)


DOI: 10.1520/C0696-19

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About ASTM

ASTM International, formerly known as the American Society for Testing and Materials (ASTM), is a globally recognized leader in the development and delivery of international voluntary consensus standards. Today, some 12,000 ASTM standards are used around the world to improve product quality, enhance safety, facilitate market access and trade, and build consumer confidence. ASTM’s leadership in international standards development is driven by the contributions of its members: more than 30,000 of the world’s top technical experts and business professionals representing 150 countries. Working in an open and transparent process and using ASTM’s advanced electronic infrastructure, ASTM members deliver the test methods, specifications, guides, and practices that support industries and governments worldwide.
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