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eLibrary > BS EN 1186-2:2022 Materials and articles in contact with foodstuffs. Plastics - Test methods for overall migration in vegetable oils >

BS EN 1186-2:2022 Materials and articles in contact with foodstuffs. Plastics - Test methods for overall migration in vegetable oils, 2022

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BS EN 1186-2:2022 Materials and articles in contact with foodstuffs. Plastics - Test methods for overall migration in vegetable oils, 2022

undefined
1 Scope
2 Normative references
3 Terms and definitions
4 Test methods [Go to Page]
4.1 Principle [Go to Page]
4.1.1 General
4.1.2 Method 1: total immersion
4.1.3 Method 2: cell
4.1.4 Method 3: fillable pouch
4.1.5 Method 4: reverse pouch
4.1.6 Method 5: filling a container
4.2 Reagents
4.3 Materials and apparatus [Go to Page]
4.3.1 General
4.3.2 Common materials and apparatus for all methods
4.3.3 Common materials for methods other than filling a container
4.3.4 Materials for method 1 (total immersion)
4.3.5 Materials for method 2 (cell)
4.3.6 Materials for method 3 (fillable pouches holder) and for the method 4 (reverse pouches holder)
4.3.7 Materials for method 5 (filling a container)
4.4 Preparation of test specimens [Go to Page]
4.4.1 General
4.4.2 Preparation of test specimens and determination of the area in contact [Go to Page]
4.4.2.1 General
4.4.2.2 Method 1: total immersion
4.4.2.3 Method 2: cell
4.4.2.4 Method 3: fillable pouch
4.4.2.5 Method 4: reverse pouch
4.4.2.6 Method 5: filling a container
4.5 Procedure [Go to Page]
4.5.1 General
4.5.2 Initial weighing of test specimens
4.5.3 Exposure to oil [Go to Page]
4.5.3.1 General
4.5.3.2 Method 1: Total Immersion and Method 4: Reverse pouch
4.5.3.3 Method 2: Cell
4.5.3.4 Method 3: Fillable Pouch
4.5.3.5 Method 5: Filling a container
4.5.3.6 Repeated exposure
4.5.4 Final weighing of test specimens
4.5.5 Extraction of absorbed oil
4.5.6 Determination of extracted oil [Go to Page]
4.5.6.1 Preparation of fatty acid methyl esters
4.5.6.2 Determination of fatty acid methyl esters
4.6 Expression of results [Go to Page]
4.6.1 General
4.6.2 Method of calculation [Go to Page]
4.6.2.1 Migration calculation in mg/dm2
4.6.2.2 Migration calculation in mg/kg
4.6.2.3 Migration calculation in mg/article
4.6.2.4 Migration calculation for materials in repeated contact with foodstuffs
4.6.3 Precision
5 Test report
Annex A (normative)Contact time and temperature tolerances
Annex B (normative)Determination of the suitability of oil as the fatty food simulant and of triheptadecanoin as the internal standard [Go to Page]
B.1 Principle
B.2 Procedure
B.3 Conclusions
Annex C (normative)Determination of the need for sample conditioning [Go to Page]
C.1 Principle
C.2 Procedure
C.3 Conclusions
C.4 Initial weighing of test specimens
C.5 Final weighing of test specimens
Annex D (normative)Determination of the need for sample conditioning and determination of the mass of moisture sensitive and/or with presence of volatiles specimens, by vacuum drying [Go to Page]
D.1 Principle
D.2 Establishing the need for conditioning of test specimens [Go to Page]
D.2.1 Procedure
D.2.2 Conclusions
D.3 Initial weighing of test specimens [Go to Page]
D.3.1 Conditioning of test specimens
D.3.2 Reconditioning of test specimens
D.4 Final weighing of test specimens
Annex E (informative)Typical chromatograms and calibration graph
Annex F (informative)Precision data [Go to Page]

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BS EN 1186-2:2022 Materials and articles in contact with foodstuffs. Plastics - Test methods for overall migration in vegetable oils, 2022

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