1. Scope

1.1 This test method describes the apparatus and general procedure for making ball-drop viscosity measurements on solutions of various cellulose derivatives. Instructions for sample preparation, solution concentration, and other details are discussed in the ASTM methods for the respective cellulose derivatives.

1.2 This test method is applicable to solutions of various cellulose derivatives having viscosities greater than 10 P, by using balls of various diameters and densities. Viscosity results are expressed preferably in poises.

1.3 In commercial practice, viscosities are often expressed in seconds using 2.38-mm (3/32-in.) stainless steel balls. When the viscosity is outside the practical range for these balls (75 to 300 P), the measurement can be made using a calibrated pipet viscometer or a different ball and calculating the observed viscosity to the corresponding time for a 2.38-mm (3/32-in.) ball, even though it is a small fraction of a second.

1.4 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.

This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

ASTM Standards

D301 Test Methods for Soluble Cellulose Nitrate

D445 Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)

D817 Test Methods of Testing Cellulose Acetate Propionate and Cellulose Acetate Butyrate

D871 Test Methods of Testing Cellulose Acetate

E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method

Keywords

ball drop; cellulose esters; viscosity; Cellulose and cellulose derivatives; Cellulose esters; Ball drop method; Viscosity--paints/related coatings/materials;

ICS Code

ICS Number Code 85.040 (Pulps)

DOI: 10.1520/D1343-95R06

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